Strain Fields’ Measurements: Novel Engineering Approach to Enrich the Characterisation of Refractories with Non-Linear Mechanical Behaviour
1 SPCTS UMR CNRS 7315, CEC, Limoges/France
2 GEMH, CEC Limoges/France
3 Prime Institute, University of Poitiers, Poitiers/France
Revision 05.05.2016, 28.09.2016
Volume 9, Issue 1, Pages 74 - 79
Abstract
The present work aimed to apply digital image correlation (DIC) used for kinematic fields’ measurements as a support for the experimental characterization of refractory materials with specific non-linear behaviour. Model and industrial materials with different degrees of flexibility were studied. The first type of materials was a single phase model flexible aluminium titanate material (AT VF) developed for academic purposes by improving the grain growth. Its non-linear mechanical behaviour was obtained thanks to the thermal expansion mismatch of its grains according to the different crystallographic axis. The second one is multi-phased magnesia based industrial materials, whose flexibility is less accentuated, and for which the non-linear mechanical behaviour is obtained thanks to the thermal expansion coefficients mismatch between spinel aggregates and magnesia matrix. In order to apply the optical methods on these materials which exhibit lower strain-to-rupture, it was necessary to optimise the accuracy of these techniques by improving experimental conditions. In the case of AT VF, DIC has been applied on four-points bending test at room temperature to underline the material asymmetric mechanical behaviour which induces a significant shift of the neutral fibre and to evaluate the relative displacement of rolls. The application of DIC has been extended to other experimental testing method such as Brazilian and wedge splitting test using the multi-phased magnesia-based materials. This highlighted fracture mechanisms (crack occurrence and propagation) and the presence of crack branching phenomenon promoted thanks to an initial microcracks network voluntary introduced by thermal expansion mismatch between the different phases so as to improve their thermal shock resistance. From displacement experimentally obtained by DIC, a finite element method updating (FEMU-U) has been developed to determine material properties.
Keywords
digital image correlation, mechanical behaviour characterization, fracture mechanisms, flexibility of refractories
References
[1] Chu, T.C.; Ranson, W.F.; Sutton, M.A.: Applications of digital-image-correlation techniques to experimental mechanics. Exp. Mech. 25 (1985) [3] 232–244 [2] Babelot, C.; et al.: Preparation and thermomechanical characterisation of aluminum titanate flexible ceramics. J. Mater. Sci. 46 (2010) 1211–1219 [3] Leplay, P.; et al.: Identification of damage and cracking behaviours based on energy dissipation mode analysis in a quasi-brittle material using digital image correlation. Int. J. Fract. 171 (2011) [1] 35–50 [4] Harmuth, H.; et al.: Investigation of the nonlinear fracture behaviour of ordinary ceramic refractory materials. Mater. Sci. Eng. A 214 (1996) [1–2] 53–61 [5] Proveti, J.; Michot, G.: The Brazilian test: a tool for measuring the toughness of a material and its brittle to ductile transition. Int. J. Fract. 139 (2006) [3] 455–460 [6] Wattrisse, B.; et al.: Analysis of strain localisation during tensile tests by digital image correlation. Exp. Mech. 41 (2001) [1] 29–39 [7] Barranger, Y.; et al.: Strain measurement by digital image correlation: Influence of two types of speckle patterns made from rigid or deformable marks. Strain 48 (2012) [5] 357–365 [8] Belrhiti, Y.; et al.: Application of optical methods to investigate the non-linear asymmetric behaviour of ceramics exhibiting large strain to rupture by four-points bending test. J. Europ. Ceram. Soc. 32 (2012) [16] 4073–4081 [9] Grédiac, M.; Hild F.: Mesures de champs et identification en mécanique des solides. Paris 2011
Copyright
Göller Verlag GmbH